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FIGURE 4 FIGURE 5 FIGURE 6 In terms of [ 15 N, 14 N 2 -DMB]-OHCbl prepared from DMB-supplemented [ 15 N]-CDMG under anaerobic conditions, the base peak shifted from m/z 673.80 ([M + 2H] 2+ ) to m/z 679.30 (Δ m/z = + 5.5 in double charged forms) in the LC-MS spectra (Figure 7), indicating a fully 15 N-labelled corrin ring and the existence of two unlabelled nitrogen atoms in the lower ligand DMB

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10.1016/j.cbi.2009.05.007 206 SinghV.SinghR.KujurP